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Characteristic API Advanced Intermediate Impurity

1,2-Cyclopentanediol, 3-[7-[[(1R,2S)-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylsulfinyl)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-5-(2-hydroxyethoxy)-, (1S,2S,3R,5S)-

CAS No.：1644461-85-7
Product No.：152-73X
Configuration：绝对构型（亚砜手性混合物）
From：降解杂质
1,2-Cyclopentanediol, 3-(2-hydroxyethoxy)-5-[7-methoxy-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-, (1S,2S,3S,5R)-

CAS No.：2024557-22-8
Product No.：152-73K
Configuration：绝对构型
From：工艺杂质
Ethanol, 2-[[(3aR,4S,6R,6aS)-6-[7-[[(1R,2S)-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]tetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-

CAS No.：274693-26-4
Product No.：152-72
Configuration：绝对构型
From：工艺杂质
Ethanol, 2-[[(3aR,4S,6R,6aS)-6-[[5-amino-6-chloro-2-(propylthio)-4-pyrimidinyl]amino]tetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-

CAS No.：376608-74-1
Product No.：152-70
Configuration：绝对构型
From：工艺杂质
Ethanol, 2-[[(3aR,4S,6R,6aS)-6-aminotetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-, (2R,3R)-2,3-dihydroxybutanedioate (1:1)

CAS No.：376608-65-0
Product No.：152-47
Configuration：绝对构型
From：工艺杂质
5-Pyrimidinamine, 4,6-dichloro-2-(propylthio)-

CAS No.：145783-15-9
Product No.：152-34
Configuration：绝对构型
From：工艺杂质
Benzeneacetic acid, α-hydroxy-, (αR)-(1R,2S)-compd. with 2-(3,4-difluorophenyl)cyclopropanamine (1:1)

CAS No.：376608-71-8
Product No.：152-19
Configuration：绝对构型
From：工艺杂质
1,2-Cyclopentanediol, 3-[7-[[(1S,2R-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-5-(2-hydroxyethoxy)-, (1R,2R,3S,5R)-

CAS No.：NA
Product No.：152-643
Configuration：绝对构型
From：工艺杂质
(1R,2R,3S,5R)-3-(7-(((1S,2S)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

CAS No.：NA
Product No.：152-73S
Configuration：绝对构型
From：工艺杂质
(1R,2R,3S,5R)-3-(7-(((1R,2R)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

CAS No.：NA
Product No.：152-73R
Configuration：绝对构型
From：工艺杂质
(1S,2S,3R,5S)-3-(7-(((1S,2S)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

CAS No.：NA
Product No.：152-73N
Configuration：绝对构型
From：工艺杂质
(1S,2S,3R,5S)-3-(7-(((1R,2R)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

CAS No.：NA
Product No.：152-73M
Configuration：绝对构型
From：工艺杂质

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Characteristic API Advanced Intermediate Impurity

1,2-Cyclopentanediol, 3-[7-[[(1R,2S)-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylsulfinyl)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-5-(2-hydroxyethoxy)-, (1S,2S,3R,5S)-

1,2-Cyclopentanediol, 3-(2-hydroxyethoxy)-5-[7-methoxy-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-, (1S,2S,3S,5R)-

Ethanol, 2-[[(3aR,4S,6R,6aS)-6-[7-[[(1R,2S)-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]tetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-

Ethanol, 2-[[(3aR,4S,6R,6aS)-6-[[5-amino-6-chloro-2-(propylthio)-4-pyrimidinyl]amino]tetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-

Ethanol, 2-[[(3aR,4S,6R,6aS)-6-aminotetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-, (2R,3R)-2,3-dihydroxybutanedioate (1:1)

5-Pyrimidinamine, 4,6-dichloro-2-(propylthio)-

Benzeneacetic acid, α-hydroxy-, (αR)-(1R,2S)-compd. with 2-(3,4-difluorophenyl)cyclopropanamine (1:1)

1,2-Cyclopentanediol, 3-[7-[[(1S,2R-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-5-(2-hydroxyethoxy)-, (1R,2R,3S,5R)-

(1R,2R,3S,5R)-3-(7-(((1S,2S)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

(1R,2R,3S,5R)-3-(7-(((1R,2R)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

(1S,2S,3R,5S)-3-(7-(((1S,2S)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

(1S,2S,3R,5S)-3-(7-(((1R,2R)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

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Characteristic APIAdvanced IntermediateImpurity

1,​2-​Cyclopentanediol, 3-​[7-​[[(1R,​2S)​-​2-​(3,​4-​difluorophenyl)​cyclopropyl]​amino]​-​5-​(propylsulfinyl)​-​3H-​1,​2,​3-​triazolo[4,​5-​d]​pyrimidin-​3-​yl]​-​5-​(2-​hydroxyethoxy)​-​, (1S,​2S,​3R,​5S)​-

1,​2-​Cyclopentanediol, 3-​(2-​hydroxyethoxy)​-​5-​[7-​methoxy-​5-​(propylthio)​-​3H-​1,​2,​3-​triazolo[4,​5-​d]​pyrimidin-​3-​yl]​-​, (1S,​2S,​3S,​5R)​-

Ethanol, 2-​[[(3aR,​4S,​6R,​6aS)​-​6-​[[5-​amino-​6-​chloro-​2-​(propylthio)​-​4-​pyrimidinyl]​amino]​tetrahydro-​2,​2-​dimethyl-​4H-​cyclopenta-​1,​3-​dioxol-​4-​yl]​oxy]​-

Ethanol, 2-​[[(3aR,​4S,​6R,​6aS)​-​6-​aminotetrahydro-​2,​2-​dimethyl-​4H-​cyclopenta-​1,​3-​dioxol-​4-​yl]​oxy]​-​, (2R,​3R)​-​2,​3-​dihydroxybutanedioat​e (1:1)

5-​Pyrimidinamine, 4,​6-​dichloro-​2-​(propylthio)​-

Benzeneacetic acid, α-​hydroxy-​, (αR)​-​(1R,​2S)​-​compd. with 2-​(3,​4-​difluorophenyl)​cyclopropanamine (1:1)

1,​2-​Cyclopentanediol, 3-​[7-​[[(1S,​2R​-​2-​(3,​4-​difluorophenyl)​cyclopropyl]​amino]​-​5-​(propylthio)​-​3H-​1,​2,​3-​triazolo[4,​5-​d]​pyrimidin-​3-​yl]​-​5-​(2-​hydroxyethoxy)​-​, (1R,​2R,​3S,​5R)​-

(1R,2R,3S,5R)-3-(7-(((1S,2S)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

(1R,2R,3S,5R)-3-(7-(((1R,2R)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

(1S,2S,3R,5S)-3-(7-(((1S,2S)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

(1S,2S,3R,5S)-3-(7-(((1R,2R)-2-(3,4-difluorophenyl)cyclopropyl)amino)-5-(propylthio)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-3-yl)-5-(2-hydroxyethoxy)cyclopentane-1,2-diol

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Characteristic API Advanced Intermediate Impurity

1,2-Cyclopentanediol, 3-[7-[[(1R,2S)-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylsulfinyl)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-5-(2-hydroxyethoxy)-, (1S,2S,3R,5S)-

1,2-Cyclopentanediol, 3-(2-hydroxyethoxy)-5-[7-methoxy-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-, (1S,2S,3S,5R)-

Ethanol, 2-[[(3aR,4S,6R,6aS)-6-[[5-amino-6-chloro-2-(propylthio)-4-pyrimidinyl]amino]tetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-

Ethanol, 2-[[(3aR,4S,6R,6aS)-6-aminotetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]-, (2R,3R)-2,3-dihydroxybutanedioate (1:1)

5-Pyrimidinamine, 4,6-dichloro-2-(propylthio)-

Benzeneacetic acid, α-hydroxy-, (αR)-(1R,2S)-compd. with 2-(3,4-difluorophenyl)cyclopropanamine (1:1)

1,2-Cyclopentanediol, 3-[7-[[(1S,2R-2-(3,4-difluorophenyl)cyclopropyl]amino]-5-(propylthio)-3H-1,2,3-triazolo[4,5-d]pyrimidin-3-yl]-5-(2-hydroxyethoxy)-, (1R,2R,3S,5R)-